ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Tampa
6712 Benjamin Road
Suite 100
Tampa, FL 33634
Tel: (813)885-7427
TestAmerica Job ID: 660-79058-1
Client Project/Site: Sediment Testing
For:
Gator Dredging
13630 50th Way North
Clearwater, Florida 33760
Attn: Kevin Davis
Authorized for release by:
3/2/2017 3:39:03 PM
Keaton Conner, Project Mgmt. Assistant
(813)885-7427
keaton.conner@testamericainc.com
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Gator Dredging
Project/Site: Sediment Testing
TestAmerica Job ID: 660-79058-1
Page 2 of 28
TestAmerica Tampa
3/2/2017
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
2
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
4
Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
5
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
22
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
25
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 27
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 28
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Sample Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID
Client Sample ID
Received
Collected
Matrix
660-79058-1
B#1
Solid
02/17/17 12:45 02/17/17 14:20
660-79058-2
B#2
Solid
02/17/17 13:00 02/17/17 14:20
660-79058-3
B#3
Solid
02/17/17 13:10 02/17/17 14:20
660-79058-4
B#4
Solid
02/17/17 13:30 02/17/17 14:20
660-79058-5
B#5
Solid
02/17/17 13:40 02/17/17 14:20
TestAmerica Tampa
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Case Narrative
Client: Gator Dredging
TestAmerica Job ID: 660-79058-1
Project/Site: Sediment Testing
Job ID: 660-79058-1
Laboratory: TestAmerica Tampa
Narrative
Job Narrative
660-79058-1
Receipt
The samples were received on 2/17/2017 2:20 PM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 24.0º C.
GC/MS Semi VOA
Method 8270D SIM: The method blank for preparation batch 660-179818 and analytical batch 660-179834 contained 1-Methylnaphthalene,
2-Methylnaphthalene and Naphthalene above the method detection limit. This target analyte concentration was less than the reporting
limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.
Surrogate recovery for the following sample was outside control limits: B#3. Evidence of matrix interference due to non-target analytes is
present; therefore, re-extraction and/or re-analysis was not performed.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries and % RPD for preparation batch 660-179818 and analytical batch
660-179834 were outside control limits for multiple analytes. The parent, MS and MSD required dilution due to high target analyte
concentration. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was within
acceptance limits.
Due to sample matrix effect on the internal standard (ISTD), a dilution was required for the following sample: B#1.
Surrogate recovery for the following sample was outside control limits: B#1. Evidence of matrix interference due to non-target analytes is
present; therefore, re-extraction and/or re-analysis was not performed.
The method blank for preparation batch 660-180058 and analytical batch 660-180065 contained Chrysene and Benzo[b]fluoranthene
above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or
re-analysis of samples was not performed.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 660-180058 and analytical batch 660-180065 were
outside control limits. Sample matrix interference is suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
The matrix spike / matrix spike duplicate (MS/MSD) precision for preparation batch 660-180058 and analytical batch 660-180065 was
outside control limits. Sample matrix interference is suspected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
TestAmerica Tampa
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Definitions/Glossary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Qualifiers
GC/MS Semi VOA
Qualifier Description
J1
Estimated value; value may not be accurate. Surrogate recovery outside of criteria.
Qualifier
U
Indicates that the compound was analyzed for but not detected.
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
V
Indicates that the analyte was detected at or above the method detection limit in both the sample and the associated method blank and the
value of 10 times the blank value was equal to or greater than the associated sample value.
Metals
Qualifier Description
U
Indicates that the compound was analyzed for but not detected.
Qualifier
I
The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤
Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R
Percent Recovery
CFL
Contains Free Liquid
CNF
Contains no Free Liquid
DER
Duplicate error ratio (normalized absolute difference)
Dil Fac
Dilution Factor
DL, RA, RE, IN
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC
Decision level concentration
MDA
Minimum detectable activity
EDL
Estimated Detection Limit
MDC
Minimum detectable concentration
MDL
Method Detection Limit
ML
Minimum Level (Dioxin)
NC
Not Calculated
ND
Not detected at the reporting limit (or MDL or EDL if shown)
PQL
Practical Quantitation Limit
QC
Quality Control
RER
Relative error ratio
RL
Reporting Limit or Requested Limit (Radiochemistry)
RPD
Relative Percent Difference, a measure of the relative difference between two points
TEF
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
TestAmerica Tampa
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Detection Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Client Sample ID: B#1
Lab Sample ID: 660-79058-1
☼
Naphthalene
RL
62
ug/Kg
MDL
8.4
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Total/NA
5
100
8270D SIM
☼
1-Methylnaphthalene
62
ug/Kg
5.0
Total/NA
5
570
8270D SIM
☼
Fluorene
62
ug/Kg
5.6
Total/NA
5
35 I
8270D SIM
☼
Phenanthrene
62
ug/Kg
27
Total/NA
5
180
8270D SIM
☼
Anthracene
62
ug/Kg
5.6
Total/NA
5
78
8270D SIM
☼
Fluoranthene
62
ug/Kg
10
Total/NA
5
970
8270D SIM
☼
Pyrene
62
ug/Kg
5.6
Total/NA
5
770
8270D SIM
☼
Benzo[a]anthracene
62
ug/Kg
5.2
Total/NA
5
310
8270D SIM
☼
Chrysene
62
ug/Kg
5.7
Total/NA
5
610
8270D SIM
☼
Benzo[b]fluoranthene
62
ug/Kg
4.9
Total/NA
5
970
8270D SIM
☼
Benzo[k]fluoranthene
62
ug/Kg
5.5
Total/NA
5
380
8270D SIM
☼
Benzo[a]pyrene
62
ug/Kg
4.8
Total/NA
5
350
8270D SIM
☼
Benzo[g,h,i]perylene
62
ug/Kg
3.4
Total/NA
5
230
8270D SIM
☼
Indeno[1,2,3-cd]pyrene
62
ug/Kg
3.3
Total/NA
5
210
8270D SIM
☼
Dibenz(a,h)anthracene
62
ug/Kg
4.0
Total/NA
5
76
8270D SIM
Arsenic
0.010
mg/L
0.0040
SPLP East
1
0.026
6010B
Barium
0.010
mg/L
0.0020
SPLP East
1
0.094
6010B
Chromium
0.010
mg/L
0.0020
SPLP East
1
0.013
6010B
Lead
0.010
mg/L
0.0022
SPLP East
1
0.054
6010B
Copper
0.010
mg/L
0.0025
SPLP East
1
0.0079 I
6010B
Zinc
0.020
mg/L
0.0050
SPLP East
1
0.022
6010B
Client Sample ID: B#2
Lab Sample ID: 660-79058-2
☼
Naphthalene
RL
8.7
ug/Kg
MDL
1.2
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Total/NA
1
I V
8.4
8270D SIM
☼
2-Methylnaphthalene
8.7
ug/Kg
1.3
Total/NA
1
2.0 I V
8270D SIM
☼
1-Methylnaphthalene
8.7
ug/Kg
0.70
Total/NA
1
12
8270D SIM
☼
Acenaphthylene
8.7
ug/Kg
0.62
Total/NA
1
2.5 I
8270D SIM
☼
Fluorene
8.7
ug/Kg
0.79
Total/NA
1
2.7 I
8270D SIM
☼
Phenanthrene
8.7
ug/Kg
3.9
Total/NA
1
49
8270D SIM
☼
Anthracene
8.7
ug/Kg
0.79
Total/NA
1
8.5 I
8270D SIM
☼
Fluoranthene
8.7
ug/Kg
1.5
Total/NA
1
210
8270D SIM
☼
Pyrene
8.7
ug/Kg
0.79
Total/NA
1
270
8270D SIM
☼
Benzo[a]anthracene
8.7
ug/Kg
0.74
Total/NA
1
120
8270D SIM
☼
Chrysene
8.7
ug/Kg
0.80
Total/NA
1
190
8270D SIM
☼
Benzo[b]fluoranthene
8.7
ug/Kg
0.68
Total/NA
1
380
8270D SIM
☼
Benzo[k]fluoranthene
8.7
ug/Kg
0.77
Total/NA
1
120
8270D SIM
☼
Benzo[a]pyrene
8.7
ug/Kg
0.67
Total/NA
1
160
8270D SIM
☼
Benzo[g,h,i]perylene
8.7
ug/Kg
0.48
Total/NA
1
74
8270D SIM
☼
Indeno[1,2,3-cd]pyrene
8.7
ug/Kg
0.47
Total/NA
1
73
8270D SIM
☼
Dibenz(a,h)anthracene
8.7
ug/Kg
0.56
Total/NA
1
23
8270D SIM
Arsenic
0.010
mg/L
0.0040
SPLP East
1
0.0041 I
6010B
Barium
0.010
mg/L
0.0020
SPLP East
1
0.020
6010B
Chromium
0.010
mg/L
0.0020
SPLP East
1
0.0083 I
6010B
Lead
0.010
mg/L
0.0022
SPLP East
1
0.017
6010B
Copper
0.010
mg/L
0.0025
SPLP East
1
0.0080 I
6010B
Zinc
0.020
mg/L
0.0050
SPLP East
1
0.022
6010B
Client Sample ID: B#3
Lab Sample ID: 660-79058-3
TestAmerica Tampa
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Client Sample ID: B#3 (Continued)
Lab Sample ID: 660-79058-3
☼
Naphthalene
RL
8.6
ug/Kg
MDL
1.2
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Total/NA
1
V
13
8270D SIM
☼
2-Methylnaphthalene
8.6
ug/Kg
1.2
Total/NA
1
53
8270D SIM
☼
1-Methylnaphthalene
8.6
ug/Kg
0.69
Total/NA
1
34
8270D SIM
☼
Acenaphthylene
8.6
ug/Kg
0.61
Total/NA
1
1.3 I
8270D SIM
☼
Acenaphthene
8.6
ug/Kg
0.65
Total/NA
1
4.3 I
8270D SIM
☼
Fluorene
8.6
ug/Kg
0.77
Total/NA
1
4.0 I
8270D SIM
☼
Phenanthrene
8.6
ug/Kg
3.8
Total/NA
1
24
8270D SIM
☼
Anthracene
8.6
ug/Kg
0.78
Total/NA
1
3.5 I
8270D SIM
☼
Fluoranthene
8.6
ug/Kg
1.4
Total/NA
1
32
8270D SIM
☼
Pyrene
8.6
ug/Kg
0.78
Total/NA
1
34
8270D SIM
☼
Benzo[a]anthracene
8.6
ug/Kg
0.72
Total/NA
1
13
8270D SIM
☼
Chrysene
8.6
ug/Kg
0.79
Total/NA
1
23
8270D SIM
☼
Benzo[b]fluoranthene
8.6
ug/Kg
0.67
Total/NA
1
40
8270D SIM
☼
Benzo[k]fluoranthene
8.6
ug/Kg
0.75
Total/NA
1
15
8270D SIM
☼
Benzo[a]pyrene
8.6
ug/Kg
0.66
Total/NA
1
20
8270D SIM
☼
Benzo[g,h,i]perylene
8.6
ug/Kg
0.47
Total/NA
1
10
8270D SIM
☼
Indeno[1,2,3-cd]pyrene
8.6
ug/Kg
0.46
Total/NA
1
9.9
8270D SIM
☼
Dibenz(a,h)anthracene
8.6
ug/Kg
0.55
Total/NA
1
2.9 I
8270D SIM
Barium
0.010
mg/L
0.0020
SPLP East
1
0.020
6010B
Chromium
0.010
mg/L
0.0020
SPLP East
1
0.0038 I
6010B
Lead
0.010
mg/L
0.0022
SPLP East
1
0.0035 I
6010B
Copper
0.010
mg/L
0.0025
SPLP East
1
0.0026 I
6010B
Zinc
0.020
mg/L
0.0050
SPLP East
1
0.012 I
6010B
Client Sample ID: B#4
Lab Sample ID: 660-79058-4
☼
Naphthalene
RL
8.7
ug/Kg
MDL
1.2
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Total/NA
1
54
8270D SIM
☼
2-Methylnaphthalene
8.7
ug/Kg
1.3
Total/NA
1
66
8270D SIM
☼
1-Methylnaphthalene
8.7
ug/Kg
0.70
Total/NA
1
49
8270D SIM
☼
Fluorene
8.7
ug/Kg
0.78
Total/NA
1
2.5 I
8270D SIM
☼
Phenanthrene
8.7
ug/Kg
3.9
Total/NA
1
32
8270D SIM
☼
Anthracene
8.7
ug/Kg
0.79
Total/NA
1
7.1 I
8270D SIM
☼
Fluoranthene
8.7
ug/Kg
1.5
Total/NA
1
100
8270D SIM
☼
Pyrene
8.7
ug/Kg
0.79
Total/NA
1
76
8270D SIM
☼
Benzo[a]anthracene
8.7
ug/Kg
0.74
Total/NA
1
29
8270D SIM
☼
Chrysene
8.7
ug/Kg
0.80
Total/NA
1
77
8270D SIM
☼
Benzo[b]fluoranthene
8.7
ug/Kg
0.68
Total/NA
1
110
8270D SIM
☼
Benzo[k]fluoranthene
8.7
ug/Kg
0.77
Total/NA
1
38
8270D SIM
☼
Benzo[a]pyrene
8.7
ug/Kg
0.67
Total/NA
1
39
8270D SIM
☼
Benzo[g,h,i]perylene
8.7
ug/Kg
0.47
Total/NA
1
61
8270D SIM
☼
Indeno[1,2,3-cd]pyrene
8.7
ug/Kg
0.47
Total/NA
1
47
8270D SIM
☼
Dibenz(a,h)anthracene
8.7
ug/Kg
0.56
Total/NA
1
14
8270D SIM
Barium
0.010
mg/L
0.0020
SPLP East
1
0.031
6010B
Chromium
0.010
mg/L
0.0020
SPLP East
1
0.0049 I
6010B
Lead
0.010
mg/L
0.0022
SPLP East
1
0.0023 I
6010B
Copper
0.010
mg/L
0.0025
SPLP East
1
0.0035 I
6010B
Zinc
0.020
mg/L
0.0050
SPLP East
1
0.0092 I
6010B
Client Sample ID: B#5
Lab Sample ID: 660-79058-5
TestAmerica Tampa
This Detection Summary does not include radiochemical test results.
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Detection Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Client Sample ID: B#5 (Continued)
Lab Sample ID: 660-79058-5
☼
Phenanthrene
RL
9.1
ug/Kg
MDL
4.0
Analyte
Result Qualifier
Unit
Dil Fac D Method
Prep Type
Total/NA
1
35
8270D SIM
☼
Anthracene
9.1
ug/Kg
0.83
Total/NA
1
10
8270D SIM
☼
Fluoranthene
9.1
ug/Kg
1.5
Total/NA
1
110
8270D SIM
☼
Pyrene
9.1
ug/Kg
0.82
Total/NA
1
81
8270D SIM
☼
Benzo[a]anthracene
9.1
ug/Kg
0.77
Total/NA
1
27
8270D SIM
☼
Chrysene
9.1
ug/Kg
0.84
Total/NA
1
82
8270D SIM
☼
Benzo[b]fluoranthene
9.1
ug/Kg
0.71
Total/NA
1
100
8270D SIM
☼
Benzo[k]fluoranthene
9.1
ug/Kg
0.80
Total/NA
1
45
8270D SIM
☼
Benzo[a]pyrene
9.1
ug/Kg
0.70
Total/NA
1
33
8270D SIM
☼
Benzo[g,h,i]perylene
9.1
ug/Kg
0.50
Total/NA
1
54
8270D SIM
☼
Indeno[1,2,3-cd]pyrene
9.1
ug/Kg
0.49
Total/NA
1
42
8270D SIM
☼
Dibenz(a,h)anthracene
9.1
ug/Kg
0.58
Total/NA
1
13
8270D SIM
Barium
0.010
mg/L
0.0020
SPLP East
1
0.046
6010B
Chromium
0.010
mg/L
0.0020
SPLP East
1
0.0062 I
6010B
Lead
0.010
mg/L
0.0022
SPLP East
1
0.0023 I
6010B
Copper
0.010
mg/L
0.0025
SPLP East
1
0.0057 I
6010B
Zinc
0.020
mg/L
0.0050
SPLP East
1
0.0097 I
6010B
TestAmerica Tampa
This Detection Summary does not include radiochemical test results.
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Client Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID: 660-79058-1
Client Sample ID: B#1
Matrix: Solid
Date Collected: 02/17/17 12:45
Percent Solids: 53.4
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
RL
MDL
Naphthalene
100
62
8.4 ug/Kg
☼ 02/22/17 16:48 02/24/17 12:22
5
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
62
9.0 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
2-Methylnaphthalene
9.0 U
62
5.0 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
1-Methylnaphthalene
570
62
4.4 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Acenaphthylene
4.4 U
62
4.7 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Acenaphthene
4.7 U
62
5.6 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Fluorene
35 I
62
27 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Phenanthrene
180
62
5.6 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Anthracene
78
62
10 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Fluoranthene
970
62
5.6 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Pyrene
770
62
5.2 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Benzo[a]anthracene
310
62
5.7 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Chrysene
610
62
4.9 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Benzo[b]fluoranthene
970
62
5.5 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Benzo[k]fluoranthene
380
62
4.8 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Benzo[a]pyrene
350
62
3.4 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Benzo[g,h,i]perylene
230
62
3.3 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Indeno[1,2,3-cd]pyrene
210
62
4.0 ug/Kg
02/22/17 16:48 02/24/17 12:22
5
☼
Dibenz(a,h)anthracene
76
2-methylnaphthalene-d10
15 J1
50 - 150
02/22/17 16:48 02/24/17 12:22
5
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
Fluoranthene-d10
35 J1
02/22/17 16:48 02/24/17 12:22
5
50 - 150
Method: 6010B - Metals (ICP) - SPLP East
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 13:57 02/24/17 09:50
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
0.010
0.0040 mg/L
02/23/17 13:57 02/24/17 09:50
1
Arsenic
0.026
0.010
0.0020 mg/L
02/23/17 13:57 02/24/17 09:50
1
Barium
0.094
0.0040
0.0010 mg/L
02/23/17 13:57 02/24/17 09:50
1
Cadmium
0.0010 U
0.010
0.0020 mg/L
02/23/17 13:57 02/24/17 09:50
1
Chromium
0.013
0.010
0.0022 mg/L
02/23/17 13:57 02/24/17 09:50
1
Lead
0.054
0.020
0.0050 mg/L
02/23/17 13:57 02/24/17 09:50
1
Selenium
0.0050 U
0.010
0.0025 mg/L
02/23/17 13:57 02/24/17 09:50
1
Copper
0.0079 I
0.020
0.0050 mg/L
02/23/17 13:57 02/24/17 09:50
1
Zinc
0.022
Method: 7470A - Mercury (CVAA) - SPLP East
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:36
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
Lab Sample ID: 660-79058-2
Client Sample ID: B#2
Matrix: Solid
Date Collected: 02/17/17 13:00
Percent Solids: 75.8
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
RL
MDL
Naphthalene
8.4 I V
8.7
1.2 ug/Kg
☼ 02/22/17 16:48 02/23/17 18:26
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.7
1.3 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
2-Methylnaphthalene
2.0 I V
8.7
0.70 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
1-Methylnaphthalene
12
8.7
0.62 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Acenaphthylene
2.5 I
8.7
0.66 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Acenaphthene
0.66 U
TestAmerica Tampa
Page 9 of 28
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Client Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID: 660-79058-2
Client Sample ID: B#2
Matrix: Solid
Date Collected: 02/17/17 13:00
Percent Solids: 75.8
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
RL
MDL
Fluorene
2.7 I
8.7
0.79 ug/Kg
☼ 02/22/17 16:48 02/23/17 18:26
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.7
3.9 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Phenanthrene
49
8.7
0.79 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Anthracene
8.5 I
8.7
1.5 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Fluoranthene
210
8.7
0.79 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Pyrene
270
8.7
0.74 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Benzo[a]anthracene
120
8.7
0.80 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Chrysene
190
8.7
0.68 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Benzo[b]fluoranthene
380
8.7
0.77 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Benzo[k]fluoranthene
120
8.7
0.67 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Benzo[a]pyrene
160
8.7
0.48 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Benzo[g,h,i]perylene
74
8.7
0.47 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Indeno[1,2,3-cd]pyrene
73
8.7
0.56 ug/Kg
02/22/17 16:48 02/23/17 18:26
1
☼
Dibenz(a,h)anthracene
23
2-methylnaphthalene-d10
68
50 - 150
02/22/17 16:48 02/23/17 18:26
1
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
Fluoranthene-d10
75
02/22/17 16:48 02/23/17 18:26
1
50 - 150
Method: 6010B - Metals (ICP) - SPLP East
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 13:57 02/24/17 09:39
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
0.010
0.0040 mg/L
02/23/17 13:57 02/24/17 09:39
1
Arsenic
0.0041 I
0.010
0.0020 mg/L
02/23/17 13:57 02/24/17 09:39
1
Barium
0.020
0.0040
0.0010 mg/L
02/23/17 13:57 02/24/17 09:39
1
Cadmium
0.0010 U
0.010
0.0020 mg/L
02/23/17 13:57 02/24/17 09:39
1
Chromium
0.0083 I
0.010
0.0022 mg/L
02/23/17 13:57 02/24/17 09:39
1
Lead
0.017
0.020
0.0050 mg/L
02/23/17 13:57 02/24/17 09:39
1
Selenium
0.0050 U
0.010
0.0025 mg/L
02/23/17 13:57 02/24/17 09:39
1
Copper
0.0080 I
0.020
0.0050 mg/L
02/23/17 13:57 02/24/17 09:39
1
Zinc
0.022
Method: 7470A - Mercury (CVAA) - SPLP East
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:37
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
Lab Sample ID: 660-79058-3
Client Sample ID: B#3
Matrix: Solid
Date Collected: 02/17/17 13:10
Percent Solids: 77.8
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
RL
MDL
Naphthalene
13 V
8.6
1.2 ug/Kg
☼ 02/22/17 16:48 02/23/17 14:55
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.6
1.2 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
2-Methylnaphthalene
53
8.6
0.69 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
1-Methylnaphthalene
34
8.6
0.61 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Acenaphthylene
1.3 I
8.6
0.65 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Acenaphthene
4.3 I
8.6
0.77 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Fluorene
4.0 I
8.6
3.8 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Phenanthrene
24
8.6
0.78 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Anthracene
3.5 I
8.6
1.4 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Fluoranthene
32
8.6
0.78 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Pyrene
34
TestAmerica Tampa
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Client Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID: 660-79058-3
Client Sample ID: B#3
Matrix: Solid
Date Collected: 02/17/17 13:10
Percent Solids: 77.8
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
RL
MDL
Benzo[a]anthracene
13
8.6
0.72 ug/Kg
☼ 02/22/17 16:48 02/23/17 14:55
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.6
0.79 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Chrysene
23
8.6
0.67 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Benzo[b]fluoranthene
40
8.6
0.75 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Benzo[k]fluoranthene
15
8.6
0.66 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Benzo[a]pyrene
20
8.6
0.47 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Benzo[g,h,i]perylene
10
8.6
0.46 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Indeno[1,2,3-cd]pyrene
9.9
8.6
0.55 ug/Kg
02/22/17 16:48 02/23/17 14:55
1
☼
Dibenz(a,h)anthracene
2.9 I
2-methylnaphthalene-d10
43 J1
50 - 150
02/22/17 16:48 02/23/17 14:55
1
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
Fluoranthene-d10
48 J1
02/22/17 16:48 02/23/17 14:55
1
50 - 150
Method: 6010B - Metals (ICP) - SPLP East
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 14:00 02/24/17 09:53
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
0.010
0.0040 mg/L
02/23/17 14:00 02/24/17 09:53
1
Arsenic
0.0040 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 09:53
1
Barium
0.020
0.0040
0.0010 mg/L
02/23/17 14:00 02/24/17 09:53
1
Cadmium
0.0010 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 09:53
1
Chromium
0.0038 I
0.010
0.0022 mg/L
02/23/17 14:00 02/24/17 09:53
1
Lead
0.0035 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 09:53
1
Selenium
0.0050 U
0.010
0.0025 mg/L
02/23/17 14:00 02/24/17 09:53
1
Copper
0.0026 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 09:53
1
Zinc
0.012 I
Method: 7470A - Mercury (CVAA) - SPLP East
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:31
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
Lab Sample ID: 660-79058-4
Client Sample ID: B#4
Matrix: Solid
Date Collected: 02/17/17 13:30
Percent Solids: 76.2
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
RL
MDL
Naphthalene
54
8.7
1.2 ug/Kg
☼ 03/02/17 08:24 03/02/17 12:13
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.7
1.3 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
2-Methylnaphthalene
66
8.7
0.70 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
1-Methylnaphthalene
49
8.7
0.62 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Acenaphthylene
0.62 U
8.7
0.66 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Acenaphthene
0.66 U
8.7
0.78 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Fluorene
2.5 I
8.7
3.9 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Phenanthrene
32
8.7
0.79 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Anthracene
7.1 I
8.7
1.5 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Fluoranthene
100
8.7
0.79 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Pyrene
76
8.7
0.74 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Benzo[a]anthracene
29
8.7
0.80 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Chrysene
77
8.7
0.68 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Benzo[b]fluoranthene
110
8.7
0.77 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Benzo[k]fluoranthene
38
8.7
0.67 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Benzo[a]pyrene
39
TestAmerica Tampa
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Client Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID: 660-79058-4
Client Sample ID: B#4
Matrix: Solid
Date Collected: 02/17/17 13:30
Percent Solids: 76.2
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
RL
MDL
Benzo[g,h,i]perylene
61
8.7
0.47 ug/Kg
☼ 03/02/17 08:24 03/02/17 12:13
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
8.7
0.47 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Indeno[1,2,3-cd]pyrene
47
8.7
0.56 ug/Kg
03/02/17 08:24 03/02/17 12:13
1
☼
Dibenz(a,h)anthracene
14
2-methylnaphthalene-d10
54
50 - 150
03/02/17 08:24 03/02/17 12:13
1
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
Fluoranthene-d10
59
03/02/17 08:24 03/02/17 12:13
1
50 - 150
Method: 6010B - Metals (ICP) - SPLP East
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 14:00 02/24/17 09:56
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
0.010
0.0040 mg/L
02/23/17 14:00 02/24/17 09:56
1
Arsenic
0.0040 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 09:56
1
Barium
0.031
0.0040
0.0010 mg/L
02/23/17 14:00 02/24/17 09:56
1
Cadmium
0.0010 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 09:56
1
Chromium
0.0049 I
0.010
0.0022 mg/L
02/23/17 14:00 02/24/17 09:56
1
Lead
0.0023 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 09:56
1
Selenium
0.0050 U
0.010
0.0025 mg/L
02/23/17 14:00 02/24/17 09:56
1
Copper
0.0035 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 09:56
1
Zinc
0.0092 I
Method: 7470A - Mercury (CVAA) - SPLP East
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:39
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
Lab Sample ID: 660-79058-5
Client Sample ID: B#5
Matrix: Solid
Date Collected: 02/17/17 13:40
Percent Solids: 73.7
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
RL
MDL
Naphthalene
1.2 U
9.1
1.2 ug/Kg
☼ 03/02/17 08:24 03/02/17 12:34
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
9.1
1.3 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
2-Methylnaphthalene
1.3 U
9.1
0.73 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
1-Methylnaphthalene
0.73 U
9.1
0.64 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Acenaphthylene
0.64 U
9.1
0.69 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Acenaphthene
0.69 U
9.1
0.82 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Fluorene
0.82 U
9.1
4.0 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Phenanthrene
35
9.1
0.83 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Anthracene
10
9.1
1.5 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Fluoranthene
110
9.1
0.82 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Pyrene
81
9.1
0.77 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Benzo[a]anthracene
27
9.1
0.84 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Chrysene
82
9.1
0.71 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Benzo[b]fluoranthene
100
9.1
0.80 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Benzo[k]fluoranthene
45
9.1
0.70 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Benzo[a]pyrene
33
9.1
0.50 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Benzo[g,h,i]perylene
54
9.1
0.49 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Indeno[1,2,3-cd]pyrene
42
9.1
0.58 ug/Kg
03/02/17 08:24 03/02/17 12:34
1
☼
Dibenz(a,h)anthracene
13
2-methylnaphthalene-d10
77
50 - 150
03/02/17 08:24 03/02/17 12:34
1
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
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Client Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Lab Sample ID: 660-79058-5
Client Sample ID: B#5
Matrix: Solid
Date Collected: 02/17/17 13:40
Percent Solids: 73.7
Date Received: 02/17/17 14:20
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Fluoranthene-d10
56
50 - 150
03/02/17 08:24 03/02/17 12:34
1
Surrogate
Dil Fac
Analyzed
Prepared
Qualifier
Limits
%Recovery
Method: 6010B - Metals (ICP) - SPLP East
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 14:00 02/24/17 10:05
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
0.010
0.0040 mg/L
02/23/17 14:00 02/24/17 10:05
1
Arsenic
0.0040 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 10:05
1
Barium
0.046
0.0040
0.0010 mg/L
02/23/17 14:00 02/24/17 10:05
1
Cadmium
0.0010 U
0.010
0.0020 mg/L
02/23/17 14:00 02/24/17 10:05
1
Chromium
0.0062 I
0.010
0.0022 mg/L
02/23/17 14:00 02/24/17 10:05
1
Lead
0.0023 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 10:05
1
Selenium
0.0050 U
0.010
0.0025 mg/L
02/23/17 14:00 02/24/17 10:05
1
Copper
0.0057 I
0.020
0.0050 mg/L
02/23/17 14:00 02/24/17 10:05
1
Zinc
0.0097 I
Method: 7470A - Mercury (CVAA) - SPLP East
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:19 02/24/17 11:44
1
Analyte
Dil Fac
Analyzed
Prepared
Unit
D
Result Qualifier
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QC Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM)
Client Sample ID: Method Blank
Lab Sample ID: MB 660-179818/1-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179834
Prep Batch: 179818
RL
MDL
Naphthalene
1.73 I
6.5
0.88 ug/Kg
02/22/17 16:48 02/23/17 10:02
1
MB MB
Analyte
Dil Fac
Analyzed
Prepared
D
Unit
Result Qualifier
1.44 I
0.95
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
2-Methylnaphthalene
0.850 I
0.53
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
1-Methylnaphthalene
0.46 U
0.46
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Acenaphthylene
0.49 U
0.49
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Acenaphthene
0.59 U
0.59
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Fluorene
2.9 U
2.9
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Phenanthrene
0.59 U
0.59
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Anthracene
1.1 U
1.1
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Fluoranthene
0.59 U
0.59
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Pyrene
0.55 U
0.55
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Benzo[a]anthracene
0.60 U
0.60
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Chrysene
0.51 U
0.51
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Benzo[b]fluoranthene
0.57 U
0.57
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Benzo[k]fluoranthene
0.50 U
0.50
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Benzo[a]pyrene
0.36 U
0.36
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Benzo[g,h,i]perylene
0.35 U
0.35
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Indeno[1,2,3-cd]pyrene
0.42 U
0.42
6.5
ug/Kg
02/22/17 16:48 02/23/17 10:02
1
Dibenz(a,h)anthracene
2-methylnaphthalene-d10
82
50 - 150
02/23/17 10:02
1
MB MB
Surrogate
02/22/17 16:48
Dil Fac
Prepared
Analyzed
Qualifier
Limits
%Recovery
84
02/22/17 16:48 02/23/17 10:02
1
Fluoranthene-d10
50 - 150
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-179818/2-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179834
Prep Batch: 179818
Naphthalene
327
211
ug/Kg
64
34 - 107
Analyte
LCS LCS
D
Unit
Result Qualifier
%Rec
Spike
Added
%Rec.
Limits
2-Methylnaphthalene
327
205
ug/Kg
63
33 - 103
1-Methylnaphthalene
327
211
ug/Kg
65
33 - 105
Acenaphthylene
327
243
ug/Kg
74
33 - 113
Acenaphthene
327
233
ug/Kg
71
33 - 110
Fluorene
327
246
ug/Kg
75
34 - 113
Phenanthrene
327
239
ug/Kg
73
33 - 114
Anthracene
327
244
ug/Kg
75
32 - 116
Fluoranthene
327
221
ug/Kg
68
31 - 113
Pyrene
327
290
ug/Kg
89
32 - 123
Benzo[a]anthracene
327
281
ug/Kg
86
37 - 126
Chrysene
327
273
ug/Kg
83
35 - 128
Benzo[b]fluoranthene
327
258
ug/Kg
79
40 - 127
Benzo[k]fluoranthene
327
263
ug/Kg
80
33 - 125
Benzo[a]pyrene
327
262
ug/Kg
80
36 - 126
Benzo[g,h,i]perylene
327
247
ug/Kg
75
40 - 122
Indeno[1,2,3-cd]pyrene
327
241
ug/Kg
74
40 - 121
Dibenz(a,h)anthracene
327
237
ug/Kg
72
40 - 120
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QC Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-179818/2-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179834
Prep Batch: 179818
2-methylnaphthalene-d10
50 - 150
Surrogate
68
LCS LCS
Qualifier
Limits
%Recovery
73
Fluoranthene-d10
50 - 150
Client Sample ID: Method Blank
Lab Sample ID: MB 660-180058/1-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 180065
Prep Batch: 180058
RL
MDL
Naphthalene
0.90 U
6.6
0.90 ug/Kg
03/02/17 08:24 03/02/17 11:27
1
MB MB
Analyte
Dil Fac
Analyzed
Prepared
D
Unit
Result Qualifier
0.96 U
0.96
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
2-Methylnaphthalene
0.54 U
0.54
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
1-Methylnaphthalene
0.47 U
0.47
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Acenaphthylene
0.50 U
0.50
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Acenaphthene
0.60 U
0.60
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Fluorene
2.9 U
2.9
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Phenanthrene
0.60 U
0.60
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Anthracene
1.1 U
1.1
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Fluoranthene
0.60 U
0.60
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Pyrene
0.56 U
0.56
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Benzo[a]anthracene
0.627 I
0.61
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Chrysene
0.853 I
0.52
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Benzo[b]fluoranthene
0.58 U
0.58
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Benzo[k]fluoranthene
0.51 U
0.51
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Benzo[a]pyrene
0.36 U
0.36
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Benzo[g,h,i]perylene
0.36 U
0.36
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Indeno[1,2,3-cd]pyrene
0.42 U
0.42
6.6
ug/Kg
03/02/17 08:24 03/02/17 11:27
1
Dibenz(a,h)anthracene
2-methylnaphthalene-d10
73
50 - 150
03/02/17 11:27
1
MB MB
Surrogate
03/02/17 08:24
Dil Fac
Prepared
Analyzed
Qualifier
Limits
%Recovery
87
03/02/17 08:24 03/02/17 11:27
1
Fluoranthene-d10
50 - 150
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-180058/2-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 180065
Prep Batch: 180058
Naphthalene
324
203
ug/Kg
63
34 - 107
Analyte
LCS LCS
D
Unit
Result Qualifier
%Rec
Spike
Added
%Rec.
Limits
2-Methylnaphthalene
324
189
ug/Kg
58
33 - 103
1-Methylnaphthalene
324
196
ug/Kg
61
33 - 105
Acenaphthylene
324
223
ug/Kg
69
33 - 113
Acenaphthene
324
217
ug/Kg
67
33 - 110
Fluorene
324
232
ug/Kg
72
34 - 113
Phenanthrene
324
231
ug/Kg
71
33 - 114
Anthracene
324
221
ug/Kg
68
32 - 116
Fluoranthene
324
221
ug/Kg
68
31 - 113
Pyrene
324
253
ug/Kg
78
32 - 123
Benzo[a]anthracene
324
254
ug/Kg
78
37 - 126
Chrysene
324
246
ug/Kg
76
35 - 128
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QC Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method: 8270D SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-180058/2-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 180065
Prep Batch: 180058
Benzo[b]fluoranthene
324
235
ug/Kg
73
40 - 127
Analyte
LCS LCS
D
Unit
Result Qualifier
%Rec
Spike
Added
%Rec.
Limits
Benzo[k]fluoranthene
324
239
ug/Kg
74
33 - 125
Benzo[a]pyrene
324
240
ug/Kg
74
36 - 126
Benzo[g,h,i]perylene
324
250
ug/Kg
77
40 - 122
Indeno[1,2,3-cd]pyrene
324
247
ug/Kg
76
40 - 121
Dibenz(a,h)anthracene
324
242
ug/Kg
75
40 - 120
2-methylnaphthalene-d10
50 - 150
Surrogate
63
LCS LCS
Qualifier
Limits
%Recovery
76
Fluoranthene-d10
50 - 150
Method: 6010B - Metals (ICP)
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-179864/7-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179893
Prep Batch: 179864
Silver
1.00
1.03
mg/L
103
80 - 120
Analyte
LCS LCS
D
Unit
Result Qualifier
%Rec
Spike
Added
%Rec.
Limits
Arsenic
1.00
0.979
mg/L
98
80 - 120
Barium
1.00
1.06
mg/L
106
80 - 120
Cadmium
1.00
1.00
mg/L
100
80 - 120
Chromium
1.00
1.04
mg/L
104
80 - 120
Lead
1.00
1.04
mg/L
104
80 - 120
Selenium
1.00
1.01
mg/L
101
80 - 120
Copper
1.00
1.04
mg/L
104
80 - 120
Zinc
1.00
1.02
mg/L
102
80 - 120
Client Sample ID: Method Blank
Lab Sample ID: LB 660-179820/1-B
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179893
Prep Batch: 179864
RL
MDL
Silver
0.0015 U
0.0040
0.0015 mg/L
02/23/17 13:57 02/24/17 09:30
1
LB LB
Analyte
Dil Fac
Analyzed
Prepared
D
Unit
Result Qualifier
0.0040 U
0.0040
0.010
mg/L
02/23/17 13:57 02/24/17 09:30
1
Arsenic
0.0020 U
0.0020
0.010
mg/L
02/23/17 13:57 02/24/17 09:30
1
Barium
0.0010 U
0.0010
0.0040
mg/L
02/23/17 13:57 02/24/17 09:30
1
Cadmium
0.0020 U
0.0020
0.010
mg/L
02/23/17 13:57 02/24/17 09:30
1
Chromium
0.0022 U
0.0022
0.010
mg/L
02/23/17 13:57 02/24/17 09:30
1
Lead
0.0050 U
0.0050
0.020
mg/L
02/23/17 13:57 02/24/17 09:30
1
Selenium
0.0025 U
0.0025
0.010
mg/L
02/23/17 13:57 02/24/17 09:30
1
Copper
0.0050 U
0.0050
0.020
mg/L
02/23/17 13:57 02/24/17 09:30
1
Zinc
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QC Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method: 6010B - Metals (ICP) (Continued)
Client Sample ID: B#2
Lab Sample ID: 660-79058-2 MS
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179893
Prep Batch: 179864
Silver
0.0015 U
1.00
1.02
mg/L
102
80 - 120
Analyte
MS MS
D
Unit
Result Qualifier
%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Arsenic
0.0041 I
1.00
0.986
mg/L
98
80 - 120
Barium
0.020
1.00
1.07
mg/L
105
80 - 120
Cadmium
0.0010 U
1.00
0.998
mg/L
100
80 - 120
Chromium
0.0083 I
1.00
1.02
mg/L
101
80 - 120
Lead
0.017
1.00
1.01
mg/L
99
80 - 120
Selenium
0.0050 U
1.00
1.01
mg/L
101
80 - 120
Copper
0.0080 I
1.00
1.02
mg/L
101
80 - 120
Zinc
0.022
1.00
1.04
mg/L
102
80 - 120
Client Sample ID: B#2
Lab Sample ID: 660-79058-2 MSD
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179893
Prep Batch: 179864
Silver
0.0015 U
1.00
1.02
mg/L
102
80 - 120
1
20
Analyte
MSD MSD
D
Unit
Result Qualifier
%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Limit
RPD
RPD
Arsenic
0.0041 I
1.00
0.990
mg/L
99
80 - 120
0
20
Barium
0.020
1.00
1.05
mg/L
103
80 - 120
1
20
Cadmium
0.0010 U
1.00
0.997
mg/L
100
80 - 120
0
20
Chromium
0.0083 I
1.00
1.02
mg/L
101
80 - 120
0
20
Lead
0.017
1.00
1.01
mg/L
99
80 - 120
0
20
Selenium
0.0050 U
1.00
1.01
mg/L
101
80 - 120
0
20
Copper
0.0080 I
1.00
1.02
mg/L
102
80 - 120
0
20
Zinc
0.022
1.00
1.04
mg/L
102
80 - 120
1
20
Method: 7470A - Mercury (CVAA)
Client Sample ID: Method Blank
Lab Sample ID: MB 660-179877/16-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179899
Prep Batch: 179877
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:00
1
MB MB
Analyte
Dil Fac
Analyzed
Prepared
D
Unit
Result Qualifier
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 660-179877/24-A
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 179899
Prep Batch: 179877
Mercury
0.00140
0.00126
mg/L
90
80 - 120
Analyte
LCS LCS
D
Unit
Result Qualifier
%Rec
Spike
Added
%Rec.
Limits
Client Sample ID: Method Blank
Lab Sample ID: LB 660-179820/1-C
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179899
Prep Batch: 179877
RL
MDL
Mercury
0.00050 U
0.00070
0.00050 mg/L
02/24/17 08:00 02/24/17 11:17
1
LB LB
Analyte
Dil Fac
Analyzed
Prepared
D
Unit
Result Qualifier
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QC Sample Results
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method: 7470A - Mercury (CVAA) (Continued)
Client Sample ID: B#3
Lab Sample ID: 660-79058-3 MS
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179899
Prep Batch: 179877
Mercury
0.00050 U
0.00140
0.00127
mg/L
91
80 - 120
Analyte
MS MS
D
Unit
Result Qualifier
%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Client Sample ID: B#3
Lab Sample ID: 660-79058-3 MSD
Matrix: Solid
Prep Type: SPLP East
Analysis Batch: 179899
Prep Batch: 179877
Mercury
0.00050 U
0.00140
0.00125
mg/L
89
80 - 120
2
20
Analyte
MSD MSD
D
Unit
Result Qualifier
%Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec.
Limits
Limit
RPD
RPD
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QC Association Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
GC/MS Semi VOA
Prep Batch: 179818
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
3546
660-79058-1
B#1
Total/NA
Solid
3546
660-79058-2
B#2
Total/NA
Solid
3546
660-79058-3
B#3
Total/NA
Solid
3546
MB 660-179818/1-A
Method Blank
Total/NA
Solid
3546
LCS 660-179818/2-A
Lab Control Sample
Total/NA
Analysis Batch: 179834
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
8270D SIM
179818
660-79058-2
B#2
Total/NA
Solid
8270D SIM
179818
660-79058-3
B#3
Total/NA
Solid
8270D SIM
179818
MB 660-179818/1-A
Method Blank
Total/NA
Solid
8270D SIM
179818
LCS 660-179818/2-A
Lab Control Sample
Total/NA
Analysis Batch: 179876
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
8270D SIM
179818
660-79058-1
B#1
Total/NA
Analysis Batch: 180056
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
8270D SIM
180058
660-79058-4
B#4
Total/NA
Solid
8270D SIM
180058
660-79058-5
B#5
Total/NA
Prep Batch: 180058
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
3546
660-79058-4
B#4
Total/NA
Solid
3546
660-79058-5
B#5
Total/NA
Solid
3546
MB 660-180058/1-A
Method Blank
Total/NA
Solid
3546
LCS 660-180058/2-A
Lab Control Sample
Total/NA
Analysis Batch: 180065
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
8270D SIM
180058
MB 660-180058/1-A
Method Blank
Total/NA
Solid
8270D SIM
180058
LCS 660-180058/2-A
Lab Control Sample
Total/NA
Metals
Leach Batch: 179820
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
1312
660-79058-1
B#1
SPLP East
Solid
1312
660-79058-2
B#2
SPLP East
Solid
1312
660-79058-3
B#3
SPLP East
Solid
1312
660-79058-4
B#4
SPLP East
Solid
1312
660-79058-5
B#5
SPLP East
Solid
1312
LB 660-179820/1-B
Method Blank
SPLP East
Solid
1312
LB 660-179820/1-C
Method Blank
SPLP East
Solid
1312
660-79058-2 MS
B#2
SPLP East
Solid
1312
660-79058-2 MSD
B#2
SPLP East
Solid
1312
660-79058-3 MS
B#3
SPLP East
Solid
1312
660-79058-3 MSD
B#3
SPLP East
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QC Association Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Metals (Continued)
Prep Batch: 179864
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
3010A
179820
660-79058-1
B#1
SPLP East
Solid
3010A
179820
660-79058-2
B#2
SPLP East
Solid
3010A
179820
660-79058-3
B#3
SPLP East
Solid
3010A
179820
660-79058-4
B#4
SPLP East
Solid
3010A
179820
660-79058-5
B#5
SPLP East
Solid
3010A
179820
LB 660-179820/1-B
Method Blank
SPLP East
Solid
3010A
LCS 660-179864/7-A
Lab Control Sample
Total/NA
Solid
3010A
179820
660-79058-2 MS
B#2
SPLP East
Solid
3010A
179820
660-79058-2 MSD
B#2
SPLP East
Prep Batch: 179877
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
7470A
179820
660-79058-1
B#1
SPLP East
Solid
7470A
179820
660-79058-2
B#2
SPLP East
Solid
7470A
179820
660-79058-3
B#3
SPLP East
Solid
7470A
179820
660-79058-4
B#4
SPLP East
Solid
7470A
179820
660-79058-5
B#5
SPLP East
Solid
7470A
179820
LB 660-179820/1-C
Method Blank
SPLP East
Solid
7470A
MB 660-179877/16-A
Method Blank
Total/NA
Solid
7470A
LCS 660-179877/24-A
Lab Control Sample
Total/NA
Solid
7470A
179820
660-79058-3 MS
B#3
SPLP East
Solid
7470A
179820
660-79058-3 MSD
B#3
SPLP East
Analysis Batch: 179893
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
6010B
179864
660-79058-1
B#1
SPLP East
Solid
6010B
179864
660-79058-2
B#2
SPLP East
Solid
6010B
179864
660-79058-3
B#3
SPLP East
Solid
6010B
179864
660-79058-4
B#4
SPLP East
Solid
6010B
179864
660-79058-5
B#5
SPLP East
Solid
6010B
179864
LB 660-179820/1-B
Method Blank
SPLP East
Solid
6010B
179864
LCS 660-179864/7-A
Lab Control Sample
Total/NA
Solid
6010B
179864
660-79058-2 MS
B#2
SPLP East
Solid
6010B
179864
660-79058-2 MSD
B#2
SPLP East
Analysis Batch: 179899
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
7470A
179877
660-79058-1
B#1
SPLP East
Solid
7470A
179877
660-79058-2
B#2
SPLP East
Solid
7470A
179877
660-79058-3
B#3
SPLP East
Solid
7470A
179877
660-79058-4
B#4
SPLP East
Solid
7470A
179877
660-79058-5
B#5
SPLP East
Solid
7470A
179877
LB 660-179820/1-C
Method Blank
SPLP East
Solid
7470A
179877
MB 660-179877/16-A
Method Blank
Total/NA
Solid
7470A
179877
LCS 660-179877/24-A
Lab Control Sample
Total/NA
Solid
7470A
179877
660-79058-3 MS
B#3
SPLP East
Solid
7470A
179877
660-79058-3 MSD
B#3
SPLP East
TestAmerica Tampa
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QC Association Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
General Chemistry
Analysis Batch: 179714
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
Moisture
660-79058-2
B#2
Total/NA
Solid
Moisture
660-79058-3
B#3
Total/NA
Solid
Moisture
660-79058-4
B#4
Total/NA
Solid
Moisture
660-79058-5
B#5
Total/NA
Analysis Batch: 179761
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Solid
Moisture
660-79058-1
B#1
Total/NA
Solid
Moisture
660-79058-1 DU
B#1
Total/NA
TestAmerica Tampa
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Lab Chronicle
Client: Gator Dredging
TestAmerica Job ID: 660-79058-1
Project/Site: Sediment Testing
Client Sample ID: B#1
Lab Sample ID: 660-79058-1
Matrix: Solid
Date Collected: 02/17/17 12:45
Date Received: 02/17/17 14:20
Leach
1312
02/21/17 20:30 GH1
179820
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Prep
3010A
179864 02/23/17 13:57 GAF
TAL TAM
SPLP East
Analysis
6010B
1
179893 02/24/17 09:50 GAF
TAL TAM
SPLP East
Leach
1312
179820 02/21/17 20:30 GH1
TAL TAM
SPLP East
Prep
7470A
179877 02/24/17 08:00 GAF
TAL TAM
SPLP East
Analysis
7470A
1
179899 02/24/17 11:36 GAF
TAL TAM
SPLP East
Analysis
Moisture
1
179761 02/21/17 06:03 AJG
TAL TAM
Total/NA
Client Sample ID: B#1
Lab Sample ID: 660-79058-1
Matrix: Solid
Date Collected: 02/17/17 12:45
Percent Solids: 53.4
Date Received: 02/17/17 14:20
Prep
3546
02/22/17 16:48 KNY
179818
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis
8270D SIM
5
179876 02/24/17 12:22 MWJ
TAL TAM
Total/NA
Client Sample ID: B#2
Lab Sample ID: 660-79058-2
Matrix: Solid
Date Collected: 02/17/17 13:00
Date Received: 02/17/17 14:20
Leach
1312
02/21/17 20:30 GH1
179820
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Prep
3010A
179864 02/23/17 13:57 GAF
TAL TAM
SPLP East
Analysis
6010B
1
179893 02/24/17 09:39 GAF
TAL TAM
SPLP East
Leach
1312
179820 02/21/17 20:30 GH1
TAL TAM
SPLP East
Prep
7470A
179877 02/24/17 08:00 GAF
TAL TAM
SPLP East
Analysis
7470A
1
179899 02/24/17 11:37 GAF
TAL TAM
SPLP East
Analysis
Moisture
1
179714 02/20/17 12:39 AJG
TAL TAM
Total/NA
Client Sample ID: B#2
Lab Sample ID: 660-79058-2
Matrix: Solid
Date Collected: 02/17/17 13:00
Percent Solids: 75.8
Date Received: 02/17/17 14:20
Prep
3546
02/22/17 16:48 KNY
179818
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis
8270D SIM
1
179834 02/23/17 18:26 MWJ
TAL TAM
Total/NA
Client Sample ID: B#3
Lab Sample ID: 660-79058-3
Matrix: Solid
Date Collected: 02/17/17 13:10
Date Received: 02/17/17 14:20
Leach
1312
02/21/17 20:30 GH1
179820
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
TestAmerica Tampa
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Lab Chronicle
Client: Gator Dredging
TestAmerica Job ID: 660-79058-1
Project/Site: Sediment Testing
Client Sample ID: B#3
Lab Sample ID: 660-79058-3
Matrix: Solid
Date Collected: 02/17/17 13:10
Date Received: 02/17/17 14:20
Prep
3010A
02/23/17 14:00 GAF
179864
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Analysis
6010B
1
179893 02/24/17 09:53 GAF
TAL TAM
SPLP East
Leach
1312
179820 02/21/17 20:30 GH1
TAL TAM
SPLP East
Prep
7470A
179877 02/24/17 08:00 GAF
TAL TAM
SPLP East
Analysis
7470A
1
179899 02/24/17 11:31 GAF
TAL TAM
SPLP East
Analysis
Moisture
1
179714 02/20/17 12:19 AJG
TAL TAM
Total/NA
Client Sample ID: B#3
Lab Sample ID: 660-79058-3
Matrix: Solid
Date Collected: 02/17/17 13:10
Percent Solids: 77.8
Date Received: 02/17/17 14:20
Prep
3546
02/22/17 16:48 KNY
179818
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis
8270D SIM
1
179834 02/23/17 14:55 MWJ
TAL TAM
Total/NA
Client Sample ID: B#4
Lab Sample ID: 660-79058-4
Matrix: Solid
Date Collected: 02/17/17 13:30
Date Received: 02/17/17 14:20
Leach
1312
02/21/17 20:30 GH1
179820
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Prep
3010A
179864 02/23/17 14:00 GAF
TAL TAM
SPLP East
Analysis
6010B
1
179893 02/24/17 09:56 GAF
TAL TAM
SPLP East
Leach
1312
179820 02/21/17 20:30 GH1
TAL TAM
SPLP East
Prep
7470A
179877 02/24/17 08:00 GAF
TAL TAM
SPLP East
Analysis
7470A
1
179899 02/24/17 11:39 GAF
TAL TAM
SPLP East
Analysis
Moisture
1
179714 02/20/17 12:25 AJG
TAL TAM
Total/NA
Client Sample ID: B#4
Lab Sample ID: 660-79058-4
Matrix: Solid
Date Collected: 02/17/17 13:30
Percent Solids: 76.2
Date Received: 02/17/17 14:20
Prep
3546
03/02/17 08:24 KNY
180058
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis
8270D SIM
1
180056 03/02/17 12:13 MWJ
TAL TAM
Total/NA
Client Sample ID: B#5
Lab Sample ID: 660-79058-5
Matrix: Solid
Date Collected: 02/17/17 13:40
Date Received: 02/17/17 14:20
Leach
1312
02/21/17 20:30 GH1
179820
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Prep
3010A
179864 02/23/17 14:00 GAF
TAL TAM
SPLP East
TestAmerica Tampa
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Lab Chronicle
Client: Gator Dredging
TestAmerica Job ID: 660-79058-1
Project/Site: Sediment Testing
Client Sample ID: B#5
Lab Sample ID: 660-79058-5
Matrix: Solid
Date Collected: 02/17/17 13:40
Date Received: 02/17/17 14:20
Analysis
6010B
02/24/17 10:05 GAF
1
179893
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
SPLP East
Leach
1312
179820 02/21/17 20:30 GH1
TAL TAM
SPLP East
Prep
7470A
179877 02/24/17 08:19 GAF
TAL TAM
SPLP East
Analysis
7470A
1
179899 02/24/17 11:44 GAF
TAL TAM
SPLP East
Analysis
Moisture
1
179714 02/20/17 12:41 AJG
TAL TAM
Total/NA
Client Sample ID: B#5
Lab Sample ID: 660-79058-5
Matrix: Solid
Date Collected: 02/17/17 13:40
Percent Solids: 73.7
Date Received: 02/17/17 14:20
Prep
3546
03/02/17 08:24 KNY
180058
TAL TAM
Type
Batch
Batch
Method
Prep Type
Lab
Analyst
Run
Prepared
or Analyzed
Batch
Number
Dilution
Factor
Total/NA
Analysis
8270D SIM
1
180056 03/02/17 12:34 MWJ
TAL TAM
Total/NA
Laboratory References:
TAL TAM = TestAmerica Tampa, 6712 Benjamin Road, Suite 100, Tampa, FL 33634, TEL (813)885-7427
TestAmerica Tampa
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Method Summary
TestAmerica Job ID: 660-79058-1
Client: Gator Dredging
Project/Site: Sediment Testing
Method
Method Description
Laboratory
Protocol
SW846
8270D SIM
Semivolatile Organic Compounds (GC/MS SIM)
TAL TAM
SW846
6010B
Metals (ICP)
TAL TAM
SW846
7470A
Mercury (CVAA)
TAL TAM
EPA
Moisture
Percent Moisture
TAL TAM
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL TAM = TestAmerica Tampa, 6712 Benjamin Road, Suite 100, Tampa, FL 33634, TEL (813)885-7427
TestAmerica Tampa
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Certification Summary
Client: Gator Dredging
TestAmerica Job ID: 660-79058-1
Project/Site: Sediment Testing
Laboratory: TestAmerica Tampa
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority
Program
EPA Region
Certification ID
Expiration Date
Florida
E84282
4
NELAP
06-30-17
Analysis Method
Prep Method
Matrix
Analyte
The following analytes are included in this report, but certification is not offered by the governing authority:
Moisture
Solid
Percent Moisture
Moisture
Solid
Percent Solids
TestAmerica Tampa
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Login Sample Receipt Checklist
Client: Gator Dredging
Job Number: 660-79058-1
Login Number: 79058
Question
Answer
Comment
Creator: Redding, Charles S
List Source: TestAmerica Tampa
List Number: 1
N/A
Radioactivity wasn't checked or is meter.
True
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
tampered with.
True
Samples were received on ice.
False
Cooler Temperature is acceptable.
Received same day of collection; chilling process
has begun.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
False
There are no discrepancies between the containers received and the COC.
Refer to Job Narrative for details.
True
Samples are received within Holding Time (excluding tests with immediate
HTs)
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/A
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
True
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
N/A
Residual Chlorine Checked.
TestAmerica Tampa
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